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| Abstract: | Urolithiasis is identified to be a major urological disorder affecting people all over the world irrespective of their age, sex and race. Urinary stone samples resected from the urinary bladders of two patients belonging to tropical region, Kollam District of Kerala State, India are investigated by using XRD,SEM, EDAX, TGA, DSC and FTIR to understand its chemical structure. Uric acid shows exothermic peak around 432°C is due to the decomposition with the evolution of CO and cracking of the remaining products. Results of analytical studies reveal that samples under investigation consist mainly in uric acid and hydrated uric acid. Hydrogen bonding exists in hydrated uric acid samples |
| Description: | Journal of Optoelectronics and Biomedical Materials Vol. 2, Issue 2, June 2010, p. 85 - 90 |
| URI: | http://dyuthi.cusat.ac.in/purl/4552 |
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| Analytical Char ... ies Of Urinary Calculi.pdf | (459.3Kb) |
| Abstract: | Urinary stones resected from urinary bladders of patients hailing from Kollam district of Kerala State, India were analyzed by SEM, XRD and by thermal analysis techniques. The analytical results indicate that, stones have different composition, i.e., calcium phosphate, calcium phosphate hydroxide and sodium calcium carbonate. Infrared spectral studies also reveal the presence of phosphates or carbonates in these samples. Further, IR spectral investigations have revealed that amorphous carbonated species are occupied in PO4 sites in calcium phosphate type stone and OH sites in calcium phosphate hydroxide sample. Thermal studies of these samples also reveal that, carbon dioxide is released from carbonated samples upon heating which is related to amount of carbon content and bond strength. Crystals with defects and irregular morphology are grown inside the urinary bladder due to variation in crystal growth conditions |
| Description: | Spectrochimica Acta Part A 77 (2010) 442–445 |
| URI: | http://dyuthi.cusat.ac.in/purl/4547 |
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| Characterizatio ... es from Southern India.pdf | (256.2Kb) |
| Abstract: | SnO2 nanocrystalline thin films were deposited on glass substrates by the spray pyrolysis technique in air atmosphere at 375, 400, 425, 450 and 500 ◦C substrate temperatures. The obtained films were characterized by using XRD. The room temperature photoluminescence (PL) spectra of these films have near band edge (NBE) and deep level emission under the excitation of 325 nm radiation. NBE PL peak intensity decreased consistently with temperatures for samples prepared at 400, 450 and 500 ◦C, while a sudden reduction in intensity is observed for the sample prepared at 425 ◦C. A similar effect was observed for the optical transmittance spectra. These effects can be explained on the basis of the change in population of oxygen vacancies as indicated by the change in a values |
| Description: | J. Phys. D: Appl. Phys. 39 (2006) 4540–4543 |
| URI: | http://dyuthi.cusat.ac.in/purl/4546 |
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| Photoluminescen ... ms on glass substrates.pdf | (148.6Kb) |
| Abstract: | ZnO thin films were coated on amorphous glass substrate at various temperatures in the range 160-500 0C by spray pyrolysis method. The as deposited films were characterised by using XRD and SEM. Wurtzite phase of ZnO was formed at a substrate temperature of 400 0C, highly oriented (002) phase was developed with respect to increase of substrate temperature from 450 to 500 0C. Morphological and growth mode of these films were analyzed with respect to structural orientation of films from wurtzite to highly (002) oriented phase. Present study reveals that substrate temperature was one of the important parameters which determine the crystalline quality, population of defects, grain size, orientation and morphology of the films |
| Description: | Journal of Optoelectronics and Biomedical Materials Vol. 5 Issue 1, January - March 2013 p. 1 - 8 |
| URI: | http://dyuthi.cusat.ac.in/purl/4562 |
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| Structural And ... Spray Pyrolysis Method.pdf | (1.201Mb) |
| Abstract: | Th(BrO3)3·H2O single crystals were grown from its aqueous solution at room temperature. Single crystal XRD, Raman and FTIR techniques were used to investigate the crystal structure. The crystal structure was solved by Patterson method. The as grown crystals are in monoclinic system with space group P21/c. The unit cell parameters are a = 12.8555(18) Å, b = 7.8970(11) Å, c = 9.0716(10) Å, = 90°, = 131.568° and = 90° and unit cell volume is 689.1(2) Å3. Z = 8, R factor is 5.9. The Raman and FTIR studies indicate the lowering of symmetry of bromate anion from C3V to C1. Hydrogen bonds with varying strengths are present in the crystal. The centrosymmetric space group P21/c of the crystal is confirmed by the non-coincidence of majority of Raman and IR bands |
| Description: | Crystal Structure Theory and Applications, 2013, 2, 70-74 |
| URI: | http://dyuthi.cusat.ac.in/purl/4561 |
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| X-Ray Crysatllo ... horium Bromate Hydrate.pdf | (592.1Kb) |
Now showing items 1-5 of 5
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